The high pressure reactor is suitable for the research application and program control of high temperature and high pressure chemical reactions in various laboratories today. The main function of the reactor is to control various conditions in the reaction process, such as pressure, temperature, volume, residence time, concentration of each reactant, reaction rate, heat transfer coefficient, stirring rate and other parameters, as well as a chemical reaction vessel as a reactant.
Stirred High Pressure Reactor
The high pressure reactor is suitable for the research application and program control of high temperature and high pressure chemical reactions in various laboratories today. The main function of the reactor is to control various conditions in the reaction process, such as pressure, temperature, volume, residence time, concentration of each reactant, reaction rate, heat transfer coefficient, stirring rate and other parameters, as well as a chemical reaction vessel as a reactant.
The vessel of Reactor is metal.
General Max. Pressure : 414 Bar (6000 psig)
General Max. Temperature : 500℃
General Capacity: 100ml~500L
Reactors are designed to select between the metal vessel & glass vessel. And these are designed to move vessel by pressure cylinder easily.
Hydrothermal (Synthesys, Reaction, Crystallization, Precipitation, Oxidation, Decomosition)
Hydrosis
Pyrolysis
Hydrogenation, Dehydrogenation
CO2 Foaming, Composite Materials
Technical Parameters
Volume | 50mL~500L |
Temp Range | -35 ~ 600℃ |
Pressure Range(Depending on the Vessel) | Vacuum ~ 413 bar |
Control Panel | Regular |
Heating | Electric heater, Jacket type |
Agitator Type | Lip seal, Mechanical seal, Magnetic drive, etc. |
Agitator RPM | 30 rpm~1750 rpm (could be upto 3,000rpm) |
Impeller Type | Paddle, SBT, PBT, Anchor, Hellical...etc. |
Material | 304SS, 316SS, Hastelloy C-276, Inconel, Titanium…etc |
Contorl Type | Manual operation or fully automatic computer control |
Closure Type | Clamp, Gland, Bolt type, Air cylinder (Automation) |
Lifter | Screw, Air cylinder, Motor lifting |
URS
№ | Parameter name | Required parameter value |
1 | System based on a high-pressure reactor with a stirrer System includes:• reactor,• condenser,• separator,• pressure regulator• liquid mass flow regulator• parameter control system• software for remote control of system parameters• frame made of aluminum profileAvailability of a lifting mechanism for the reactor: pneumatic drivePlacement: floor with wheelsets | |
2 | Reactor, pc. | 1 |
2.1 | Volume, L. | 2 |
2.2 | Max. operation pressure, bar | 300 |
2.3 | Max. pressure temperature, оС | 450 |
2.4 | Material of construction of reactor | T316SS or analog |
2.5 | Stirrer design | overhead drive direct drive (not belt) |
2.6 | Adjustable rotation speed of the mixing element, rpm, not less | 500 |
2.7 | Mixing element motor power, W, not less | 180 |
2.8 | Electric heating power, not less | 4 kW |
2.9 | Ports: | Cooling coil: 1/4" ports;Valve (free): 1/4";Gas supply valve with deep tube: 1/4";Bleed valve: 1/4";Bottom drainvalve: 3/8"; |
2.10 | Pressure transducer | Availability, up to 300 bar |
2.11 | Pressure gauge | Availability, scale from 0 to 300 bar |
2.12 | Thermocouple type "K" and thermowell | Availability |
2.13 | Sealing element type | Teflon (PTFE) and reinforced graphite flat gasket |
3 | Condenser | 1 |
3.1 | Type of condenser | Shell and tube for liquid coolant |
3.2 | Max. pressure, bar | 300 |
3.3 | Max. temperature, оС | 300 |
3.4 | Maintaining pipeline temperature from reactor to condenser | Using electric heating |
3.5 | Material of construction of condenser | T316SS or analog |
4 | Pressure regulator | 1 |
4.1 | Type of regulation | Manual, "up to yourself" |
4.2 | Maximum temperature, оС, not less | 200 |
4.3 | Max. pressure, bar, not less | 300 |
4.4 | Material of construction | T316SS or analog |
5 | Separator | 1 |
5.1 | Volume, L. | 1 |
5.2 | Working pressure, bar | 10 |
5.3 | Working temperature, оС | 100 |
5.4 | Temperature control type | Jacket for liquid heat and coolant |
5.5 | Material of construction | T316SS or analog |
6 | Mass flow regulator | 1 |
6.1 | Maximum flow, grams per hour, not less | 10 000 |
6.2 | Minimum flow, grams per hour, not less | 1 000 |
6.3 | Max. pressure, bar, not less | 200 |
6.4 | Connection interfaces | RS232/Modbus |
6.5 | Max. temperature, оС, not less | 60 |
6.6 | Input and output ports | 1/4" |
7 | Сontrol system | 1 |
7.1 | Digital temperature controller (PID); | Availability |
7.2 | digital controller of overheating temperature parameters | Availability |
7.3 | digital indicator for monitoring pressure parameters | Availability |
7.4 | digital RPM (rpm) controller (stirrer rotation speed); | Availability |
7.5 | Fluid flow | Availability |
7.6 | emergency warning and shutdown system | Availability |
7.7 | Power supply | 220 V/1 phase/50Hz |
8 | Software for remote system management- The ability to continuously monitor and record the main technological parameters, must be equipped with a system for monitoring and controlling the operating parameters of the units (equipment) of the installation (temperatures, pressures, etc.), with this information displayed on the operator's HMI panel;- The system must ensure the collection of archival data and the presentation of trends based on current parameter data. Functional:- presence of a mnemonic diagram;- availability of a chart of key indicators in real time (temperature, pressure, stirrer speed, flow);- possibility of step-by-step temperature changes over time (cyclogram);- the ability to upload to a settlement document-table (txt, xls, nl);- availability of notification and emergency shutdown functions in case of malfunctions- availability of communication with the autonomous control panel via at least a 4-channel galvanically isolated bridge of the USB interface to RS interfaces; - the strength of galvanic isolation is at least 1000V;- work via USB 2.0 Full-speed protocol or equivalent.- selection of the interface type (RS232, RS422, RS485) for each channel must be carried out using internal jumpers;- the ability to use internal matching resistances in each channel using jumpers: availability;- the presence of information exchange indicators for each channel in the form of green and yellow LEDs on the front panel for the operator to quickly understand the equipment status;- the ability to enable or disable any of the channels using special commands from the computer;Availability of connectors for connecting to peripheral equipment and PC. | Availability |
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